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Assignment of primary and secondary amide carbonyl resonances in carbon-13 NMR

โœ Scribed by Richard A Newmark; James R Hill


Publisher
Elsevier Science
Year
1976
Weight
319 KB
Volume
21
Category
Article
ISSN
0022-2364

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## Abstract Carbonyl carbons in peracetylated saccharides are coupled via threeโ€ and twoโ€bond couplings with ring protons and acetyl methyl protons, respectively. Using their mean values, the optimum setting for 2D heterocorrelated experiments (Freemanโ€“Morris and COLOC sequences) designed for the a