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Assay procedure for spectrophotometric determination of dextroamphetamine sulfate and amobarbital formulated into timed-release capsules

✍ Scribed by Fabrizio De Fabrizio


Publisher
John Wiley and Sons
Year
1972
Tongue
English
Weight
208 KB
Volume
61
Category
Article
ISSN
0022-3549

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✦ Synopsis


An analytical method is presented for the quantitative spectrophotometric determination of a combination of dextroamphetamine sulfate and amobarbital blended in long-acting pellets. The powdered mixture is dissolved in 50% ethanol, and the solution is poured onto an alginic acid column which holds dextroamphetamine. Amobarbital, which passes through the column with the alcoholic washings, is collected in a 1Wml. volumetric flask. The assay technique offers a rapid and accurate determination of the two therapeutically active ingredients. Synthetic mixtures were analyzed by the proposed method, and recovery was 98-101 %.

Keyphrases 0 Amobarbital-dextroamphetamine sulfate timed-release formulations-GLC separation, UV spectrophotometric