Assay of Malondialdehyde in Biological Fluids by Gas Chromatography-Mass Spectrometry
โ Scribed by H.C. Yeo; H.J. Helbock; D.W. Chyu; B.N. Ames
- Publisher
- Elsevier Science
- Year
- 1994
- Tongue
- English
- Weight
- 436 KB
- Volume
- 220
- Category
- Article
- ISSN
- 0003-2697
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๐ SIMILAR VOLUMES
A gas chromatographic method is described for the quantification of free and total malondialdehyde (MDA) in biological materials. The procedure involves derivatization of the analyte with 2,4,6-trichlorophenylhydrazine, extraction with n-hexane, and separation of the cyclic derivatization product on
A method to determine free and total (free and bound) malondialdehyde (MDA) in fresh human plasma, or in rat liver microsomes, using selected ion monitoring (SIM) gas chromatography-mass spectrometry in the electron impact mode was set up. The dideuterated internal standard, 3-hydroxy[1,3-2 H 2 ]-2-