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As4S5N10–A Diaminosulfane Derivative with Two Bicyclic Arsino Sulfur Diimides

✍ Scribed by Prof. Dr. Max Herberhold; Dr. Karlheinz Guldner; Prof. Dr. Alfred Gieren; Dipl.-Phys. Catalina Ruiz-Pérez; Dr. Thomas Hübner


Publisher
John Wiley and Sons
Year
1987
Tongue
English
Weight
237 KB
Volume
26
Category
Article
ISSN
0044-8249

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✦ Synopsis


OS(CO)~CI( PHPh)( PPhJ2] [W(=CCMe3)Cl2( PHPh)(PEt,),] 3 4

The synthetic utility of magnesium phosphido reagents in gaining access to other metal phosphido complexes is being investigated. Interestingly, reaction of 5 with 1 gave the known diphosphene complex 6"" rather than the expected phosphido [NiCl2I(PR2CH2)d + IMg(PHPh)21 -5 1 [Ni(q-Ph-P= P-Ph)(( PR,CH,)& 6