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Aryl H- Phosphonates. 12. Synthetic and 31 P NMR Studies on the Preparation of Nucleoside H- Phosphonothioate and Nucleoside H- Phosphonodithioate Monoesters

✍ Scribed by Cieślak, Jacek; Jankowska, Jadwiga; Stawiński, Jacek; Kraszewski, Adam

Book ID
125418657
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
122 KB
Volume
65
Category
Article
ISSN
0022-3263

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Aryl Hphosphonates. 8. Simple and effic
Aryl Hphosphonates. 8. Simple and efficient method forv the preparation of nucleoside Hphosphonothioate monoesters
✍ Inger Kers; Annika Kers; Jacek Stawiński; Adam Kraszewski 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 257 KB

An efficient method for the preparation of nucleoside 3'-H-phosphonothioate monoesters was developed. It consists of phosphonylation of suitably protected nucleosides with diphenyl H-phosphonate to produce nucleoside phenyl H-phosphonates, followed by their sulfhydrolysis with hydrogen sulfide.