and the supernatant decanted. Water (10 mL) was added to resuspend the precipitate, which was shaken vigorously and again centrifuged. After decanting, acetone was added to the precipitate which was again shaken vigorously and centrifuged. This was repeated once more, after which the precipitate was
[(arene)Rh(cod)]+ Complexes as Catalysts for [5+2] Cycloaddition Reactions
β Scribed by Paul A. Wender; Travis J. Williams
- Publisher
- John Wiley and Sons
- Year
- 2002
- Tongue
- English
- Weight
- 131 KB
- Volume
- 114
- Category
- Article
- ISSN
- 0044-8249
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π SIMILAR VOLUMES
The first heterogeneous catalyst which affords polymerization of substituted acetylenes into readily available high molecular weight polymers is reported. The catalyst (Rh/PBI) has been prepared by supporting di-m-chlorobis(h 4 -cycloocta-1,5-diene)dirhodium(i), [Rh(cod)Cl] 2 , on commercial polyben
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