Arene–Perfluoroarene Interactions as Phy
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Andreas F. M. Kilbinger; Robert H. Grubbs
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Article
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2002
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John Wiley and Sons
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English
⚖ 103 KB
In a typical synthesis, Ni(NO 3 ) 2 ¥ 6 H 2 O (1 mmol) was heated with Na 2 (fum) (1 mmol) in water (15 mL) at 170 8C for 24 h in a teflon-lined steel vessel. Overnight cooling of the vessel results in a microcrystalline green solid along with single crystals (65 % yield) suitable for X-ray diffract