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Aqua­bis­(tetra­hydro­furan)­hexakis­(tri­chloro­acetato)copper(II)­diiron(III) hexane solvate

✍ Scribed by Ng, Seik Weng

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
196 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the oxo-centered title compound, [CuFe 2 O(C 2 Cl 3 O 2 ) 6 -(C 4 H 8 O) 2 (H 2 O)]ÁC 6 H 14 , the central O atom is linked to the three metal atoms, each of which is linked to four trichloroacetate anions. The Fe atoms are coordinated by a tetrahydrofuran molecule and the Cu atom by a water molecule. Two trimetallic units are linked by a pair of hydrogen bonds across a center of inversion into a dimeric entity.

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Single-crystal X-ray study T = 163 K Mean '(C±C) = 0.007 A Ê Disorder in main residue R factor = 0.039 wR factor = 0.109 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Aqua­bis­(tetra­hydro­furan)­hexakis­(tri­fluoro­acetato)(μ3-oxo)­zinc(II)­diiron(III)
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Single-crystal X-ray study T = 163 K Mean '(C±C) = 0.008 A Ê Disorder in main residue R factor = 0.042 wR factor = 0.119 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.