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Applications of 27Al multiple quantum magic angle spinning NMR to aluminophosphate molecular sieves

✍ Scribed by Philippe R. Bodart; Jean paul Amoureux; Marek Pruski; Alain Bailly; Christian Fernandez

Publisher: John Wiley and Sons
Year: 1999
Tongue: English
Weight: 102 KB
Volume: 37
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(199912)37:13<s69::aid-mrc533>3.0.co;2-8

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✦ Synopsis

The advantages and drawbacks of various techniques that utilize multiple quantum magic angle spinning (MQMAS) NMR for studying molecular sieves and related materials are reviewed. The techniques include z-filtered MQMAS with rotor synchronization, MQMAS with cross-polarization and MQMAS with REDOR. Several methods of recovering quantitative intensities in MQMAS spectra are discussed. Examples of applications include studies of various types of aluminophosphate.

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