✦ LIBER ✦
Application of modified selective polarization transfer experiments to the structural analysis of β-silylated silyl enol ethers by 1H, 13C and 29Si NMR
✍ Scribed by Vincent Baudrillard; Daniel Davoust; Gerard Ple
- Publisher
- John Wiley and Sons
- Year
- 1994
- Tongue
- English
- Weight
- 466 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Abstract
The ^1^H, ^13^C and ^29^Si NMR spectral characteristics of β‐silylated silyl enol ethers were determined. ^n^J(Si, H) measurements (2 < n < 4) were achieved from selective polarization transfer experiments with selective decoupling during acquisition. ^1^H,^29^Si two‐dimensional heteronuclear correlation confirmed the positions of the silylated groups in the molecules.