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Application of High Temperature High Resolution Gas Chromatography to Crude Extracts of Propolis

✍ Scribed by dos Santos Pereira, Alberto ;Pinto, Angelo C. ;Nobrega Cardoso, Jari ;Radler de Aquino Neto, Francisco ;Freiman de Souza Ramos, Mônica ;Dellamora-Ortiz, Gisela M. ;Pereira dos Santos, Elisabete

Publisher
John Wiley and Sons
Year
1998
Tongue
English
Weight
64 KB
Volume
21
Category
Article
ISSN
0935-6304

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✦ Synopsis

The underivatized acetone and hexane fractions from propolis samples (predominant flora Citrus spp. and Vernonia polyanthes) were analyzed by HT-HRGC (high temperature high resolution gas chromatography) and HT-HRGC coupled to mass spectrometry (HT-HRGC-MS). Several compounds, including flavonoid aglycones, phenolic acids, and high molecular weight compounds were characterized in crude extracts by HT-HRGC-MS. HT-HRGC and HT-HRGC-MS were shown to be quick and informative tools for rapid analysis of crude extracts without need for prior derivatization and purification.

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