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Application of amino acid type-specific 1H- and 14N-labeling in a 2H-, 15N-labeled background to a 47

โœ Scribed by Mark J.S. Kelly; Cornelia Krieger; Linda J. Ball; Yihua Yu; Gerald Richter; Peter Schmieder; Adelbert Bacher; Hartmut Oschkinat

Book ID
110262676
Publisher
Springer Netherlands
Year
1999
Tongue
English
Weight
91 KB
Volume
14
Category
Article
ISSN
0925-2738

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Enzymatic synthesis of specifically 2H-l
Enzymatic synthesis of specifically 2H-labelled L-glutamic acids and 2H-, 15N-, 13C-labelled L-glutamines on a preparative scale
โœ A. Ogrel; I. A. Vasilenko; J. Lugtenburg; J. Raap ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 707 KB

## Abstract In this paper we report the preparation of specifically ^2^Hโ€labelled Lโ€glutamic acids and ^2^Hโ€, ^15^Nโ€, ^13^Cโ€labelled Lโ€glutamines on the gram scale. The products obtained have high isotope enrichment (>98%) and high optical purity. The synthetic schemes allow the specific isotope en