Anthracyclinone Ring C Synthesis via Che
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Prof. Dr. Karl Heinz Dötz; Dr. Michael Popall
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Article
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1987
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John Wiley and Sons
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English
⚖ 335 KB
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The generation of I and their reactions with acid chlorides were performed in one flask as typified in the following example (reaction 3 in Table I). A mixture of Zn-Cu couple [I71 ( I 10 mg, 1.7 mmol) and 3-iodopropyl phenyl ketone (356 mg, 1.3 mmol) in dry benzene (4 mL) and HMPA (0.5 mL) was stir