In the structure of the title compound, C 17 H 17 N, the two molecules in the asymmetric unit are confined to distinct layers, one for each type of molecule. The layers differ in the orientation, relative to the edges of the unit cell, of the molecules within them.
(Anthracen-9-ylmethyl)diethylamine at 100 K
✍ Scribed by Howie, R. Alan ;Kindness, Andrew ;McKay, Michael G. ;Maguire, Glenn E. M.
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 260 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê Disorder in main residue R factor = 0.077 wR factor = 0.208 Data-to-parameter ratio = 16.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 240 K Mean '(C±C) = 0.003 A Ê R factor = 0.038 wR factor = 0.085 Data-to-parameter ratio = 25.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.002 A Ê R factor = 0.045 wR factor = 0.148 Data-to-parameter ratio = 16.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
A Z arrangement of substituents about the carboxylate C-O bond causes a syn positioning of the carbonyl O atom and the heterocyclic part of the title compound, C 18 H 15 NO 3 S. The carboxylate entity is inclined by À28.1 (3) to the phenyl group. The planes of the thiazol-2(3H)-thione subunit and th