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Ansa-Cycloheptatrienyl–Cyclopentadienyl Complexes

✍ Scribed by Matthias Tamm; Andreas Kunst; Thomas Bannenberg; Eberhardt Herdtweck; Peter Sirsch; Cornelis J. Elsevier; Jan M. Ernsting

Publisher
John Wiley and Sons
Year
2004
Tongue
English
Weight
210 KB
Volume
116
Category
Article
ISSN
0044-8249

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The half-sandwich titanium trimethyl complex (η 5 -C 5 H 4 CMe 2 Ar)TiMe 3 (Ar = 3,5-Me 2 C 6 H 3 ) reacts with the Lewis acid B(C 6 F 5 ) 3 to give the ionic Ti IV ansa-cyclopentadienyl-arene complex [(η 5 ,η 6 -C 5 H 4 CMe 2 Ar)TiMe 2 ]-[MeB(C 6 F 5 ) 3 ]. In bromobenzene solvent, addition of more