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ANOMALOUS EXCHANGE KINETICS OF PEPTIDE AMIDE PROTONS IN AQUEOUS SOLUTIONS

✍ Scribed by KRAUSS, ERIC M. ;COWBURN, DAVID

Book ID
115097685
Publisher
Wiley (Blackwell Publishing)
Year
2009
Tongue
English
Weight
351 KB
Volume
17
Category
Article
ISSN
0367-8377

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We have used a modified version of a previously proposed technique, MEXICO [Gemmecker et al. (1993) J. Am. Chem. Soc., 115, 11620], and improved data analysis procedures in order to measure rapid hydrogen exchange (HX) rates of amide protons in peptides labeled only with 15N. The requirement of 13C-