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Anodic oxidations. IV. Electrochemical oxidation of 2,5-dimethylthiophene

โœ Scribed by Yoshida, Kunihisa; Saeki, Tatsushi; Fueno, Takayuki

Book ID
126471540
Publisher
American Chemical Society
Year
1971
Tongue
English
Weight
724 KB
Volume
36
Category
Article
ISSN
0022-3263

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A series of [4 + 21 cycloadditions with 2,Sdimethylthiophene oxide (2), generated in situ by peracid oxidation of 2,Sdimethylthiophene (l), are described. In all cases the syn adduct (with respect to the sulfoxide oxygen) is formed exclusively. Recently the x-facial diastereoselectivity encountered