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Analytical possibilities of microelectrode use for stripping voltammetry

✍ Scribed by Frank-Michael Matysik; Petra Gläser; Gerhard Werner

Book ID
112292101
Publisher
Springer
Year
1994
Tongue
English
Weight
295 KB
Volume
349
Category
Article
ISSN
1618-2650

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Using a copper microelectrode of Ç5-mm diameter, the concentration of Se(IV) was determined by cathodic stripping voltammetry either from HClO 4 (0.1 M) or from NaClO 4 (0.1 M) supporting electrolytes. The preconcentration time of 15 s was chosen as optimal, and calibration graphs were constructed f