𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Analysis of volatiles in dehydrated carrot samples by solid-phase microextraction followed by GC-MS

✍ Scribed by Ana Cristina Soria; Jesús Sanz; Mar Villamiel

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
469 KB
Volume
31
Category
Article
ISSN
1615-9306

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

A solid‐phase microextraction (SPME)‐based method for the GC‐MS analysis of volatiles in dehydrated carrot root samples has been developed and the effect of the most important factors (fibre coating, extraction temperature, equilibrium time and extraction time) on the fractionation of different volatiles has been studied. GC‐MS chromatograms showed terpenoids relevant to carrot aroma such as α‐pinene, sabinene, β‐myrcene, limonene, γ‐terpinene, terpinolene, trans‐caryophyllene and β‐bisabolene, and several furan derivatives whose origin is discussed in this paper. As an example of application, this methodology has been used for the characterization of volatile composition of industrially dehydrated carrots. SPME followed by GC‐MS is shown as an affordable, fast and solvent‐free technique which can be performed with low sample amounts and be easily implemented at an industry for quality control purposes.

📜 SIMILAR VOLUMES

Fully automated determination of N-nitro
Fully automated determination of N-nitrosamines in environmental waters by headspace solid-phase microextraction followed by GC–MS–MS
✍ Anna Llop; Francesc Borrull; Eva Pocurull 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 200 KB 👁 1 views

## Abstract A fully automated method for determining nine Environmental Protection Agency __N__‐nitrosamines in several types of environmental waters at ng/L levels is presented. The method is based on a headspace solid‐phase microextraction followed by GC–MS–MS using chemical ionization. Three dif

Determination of volatile organic acids
Determination of volatile organic acids in tobacco by single-drop microextraction with in-syringe derivatization followed by GC-MS
✍ Yunfei Sha; Jiaoran Meng; Yichun Zhang; Chunhui Deng; Da Wu 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 155 KB 👁 1 views

## Abstract In this work, the novel technique based on headspace single‐drop microextraction with in‐syringe derivatization followed by GC‐MS was established to determine the volatile organic acids in tobacco. The parameters for headspace single‐drop microextraction and in‐syringe derivatization we

Analysis of organic compounds in environ
Analysis of organic compounds in environmental samples by headspace solid phase microextraction
✍ Zhang, Zhouyao ;Pawliszyn, Janusz 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 English ⚖ 474 KB 👁 1 views

## Abstract The analysis of samples contaminated by organic compounds is an important aspect of environmental monitoring. Because of the complex nature of these samples, isolating target organic compounds from their matrices is a major challenge. A new isolation technique, solid phase microextracti

Determination of methylmercury in fish a
Determination of methylmercury in fish and aqueous samples using solid-phase microextraction followed by gas chromatography–atomic fluorescence spectrometry
✍ Yong Cai; Sugunya Monsalud; Kenneth G. Furton; Rudolf Jaffé; Ronald D. Jones 📂 Article 📅 1998 🏛 John Wiley and Sons 🌐 English ⚖ 91 KB 👁 2 views

An analytical method is described for methylmercury determination in fish and aqueous samples using solid-phase microextraction (SPME) followed by gas chromatography-atomic fluorescence spectrometry (GC-AFS). The procedure involves aqueous-phase derivatization of methylmercury species with sodium te