Analysis of volatile sesquiterpenoids in environmental and geological samples

✍ Scribed by Elias, Valdimir O. ;Simoneit, Bernd R. T. ;Cardoso, Jari N.

• Publisher: John Wiley and Sons
• Year: 1997
• Tongue: English
• Weight: 479 KB
• Volume: 20
• Category: Article
• ISSN: 0935-6304
• DOI: 10.1002/jhrc.1240200602

✦ Synopsis

Abstract

In order to evaluate vloatile compounds, especiallly sesquiter‐penoids, in environmental and geological samples a method was penoids, in environmental and geological samples a method was required to characterize these components when they occur at low concentrations. After fractionation of the total sample extracts by TLC the aliphatic fractions were analyzed by HRGC AND THE kovats indices of all resolved peaks were calculated and comkpared with indices of all resolved peaks were calculated and compared with those obtained for commercial standards. As final step, the fractions were analyzed by HRGC‐MS and structures confirmed by comparison of their mass spectra with those of certified sesuiterpene standards. Additionally sesquiterpenoids present in the dissolved phase in water samples were concentrated by solid phase extraction using XAD‐2 resin. In this initial study, recovery tests with the resin were carried out in order to evaluate its performance rather than validating the methodology.