Analysis of sludge extracts by high resolution GC with selective detectors
β Scribed by Lopez-Avila, Viorica
- Book ID
- 102344404
- Publisher
- John Wiley and Sons
- Year
- 1980
- Tongue
- English
- Weight
- 310 KB
- Volume
- 3
- Category
- Article
- ISSN
- 0935-6304
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β¦ Synopsis
Abstract
Combination of various GC detectors by using a Varian effluent splitter with glass capillary columns has been found to be a rapid procedure for profiling organics extracted from sludges and river sediments. The selectivity and the increased sensitivity of the thermionic nitrogenβphosphorus detector (TSD), the electron capture detector (ECD), and the flame photometric detector (FPD) over the flame ionization detectors (FID) or mass spectrometers allow the detection of compounds present at trace levels without need for extensive sample cleanup. Furthermore, the combination of two selective detectors may supplement the information with regard to the chemical functionalities required for structure elucidation.
π SIMILAR VOLUMES
## Abstract The use of a photoionization detector (PID) coupled to a glass capillary gas chromatography (GC^2^) separation system for the detection of carcinogenic nitrosamines was investigated. The components analyzed gave a linear response with a lower detection limit of 50 to 100 pg with the 10.