Analysis of proton NMR spectra of 1-phospha-2,6-dioxacyclohexanes
✍ Scribed by D.W White; G.K McEwen; R.D Bertrand; J.G Verkade
- Publisher
- Elsevier Science
- Year
- 1971
- Weight
- 721 KB
- Volume
- 4
- Category
- Article
- ISSN
- 0022-2364
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## Abstract The high‐resolution proton‐coupled ^13^C NMR spectra of 2‐chloro‐ and 2‐phenyl‐4‐methyl‐1,3,2‐dithiarsolane and 2‐chloro‐ and 2‐phenyl‐1,3,2‐dithiarsolane have been obtained and completely analysed. The spectral analysis has provided all the ^13^C chemical shifts and ^13^C^1^H coupling
Complete proton and carbon NMR assignments were made for five 2-(2X-pbenyl)thiophenes (X = NH, , NO,, COOH, Br), four 2,5diphenylbeterocycles (thiophene, furan and N-methyl-and N-phenylpyrrole) and Nphenylpyrrole using HETCOR, COSY, XCORFE and, in one case, NOESY 2D NMR techniques. In the first set