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Analysis of low molecular weight plant phenolics by thermospray liquid chromatography/mass spectrometry

โœ Scribed by Guido C Galletti; John Eagles; F Alfred Mellon


Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
316 KB
Volume
59
Category
Article
ISSN
0022-5142

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โœฆ Synopsis


Abstract

High performance liquid chromatographyโ€mass spectrometry using a thermospray interface and discharge ionisation has been conducted on a group of plant phenolic standards and on a wheat straw acid hydrolysate. Protonated molecules, [M + H]^+^, were observed for the phenolic standards and it was possible to identify several phenolic compounds in the hydrolysate. These results indicate that thermospray HPLC/MS has potential as a technique for determining the presence of useful marker compounds which are indicative of the progress of the lignification during plant growth.


๐Ÿ“œ SIMILAR VOLUMES


Wine phenolicsโ€”analysis of low molecular
โœ Marie-Hรฉlรจne Salagoรฏty-Auguste; Alain Bertrand ๐Ÿ“‚ Article ๐Ÿ“… 1984 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 372 KB

Low molecular weight phenolic compounds were separated by high performance liquid chromatography on hydrocarbon-bonded reverse phase packings, with a water-methanol elution gradient. Phenolic compounds were extracted from wine with ethyl acetate. A first extraction at pH 7 enabled isolation of neutr