The separation of mixed mono-, di-, and triglycerides by capillary supercritical fluid chromatography is described. The separations were performed at low operating temperatures, using a carbon dioxide mobile phase, a conventional flame ionization detector, and two different stationary phases, DB-5 (
Analysis of commercial dyes by capillary column supercritical fluid chromatography
โ Scribed by Jackson, Wm. P. ;Later, D. W.
- Publisher
- John Wiley and Sons
- Year
- 1986
- Tongue
- English
- Weight
- 274 KB
- Volume
- 9
- Category
- Article
- ISSN
- 0935-6304
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โฆ Synopsis
High resolution separations of selected commercial azo, aniline, and anthraquinone dyes by capillary column supercritical fluid chromatography (SFC) are demonstrated. Supercritical n-pentane was used as a mobile phase and provided efficient separations of multi-functional, polar disperse dyes with molecular weights up to approximately 700 daltons.
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Newly developed perfluorinated polyethers, HOCH O CF O CF 2 2 p 2 . x ลฝ . CF O CH OH Z-Dols , were separated using packed capillary column supercrit-2 q 2 ลฝ . ical fluid chromatography SFC . A fluorocarbon-bonded stationary phase, Fluofix ลฝ . 120N 5 m and 120 A , was used as a packing material and
## Abstract Lubricating oil additives have been analyzed by supercritical fluid chromatography on open tubular and packed capillary columns. Carbon dioxide and modified carbon dioxide were used as mobile phases and detection was accomplished by flame ionization and micro UV. Rapid and efficient ana
Capillary supercritical fluid chromatography was performed using solvent-vented injection in conjunction with a thermionic ionization detector. Mixtures of organo-nitrogen and phosphorus containing agrochemicals were chromatographed and detection of low picogram quantities was observed.