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Analysis of 1H and 13C NMR Spectra of cis- and trans-10-Chlorodecal-2-ones by 2D NMR Techniques

✍ Scribed by G. Di Maio; C. Iavarone; L. M. Migneco; E. Vecchi

Publisher: John Wiley and Sons
Year: 1996
Tongue: English
Weight: 437 KB
Volume: 34
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(199601)34:1<18::aid-omr838>3.0.co;2-r

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✦ Synopsis

The 'H and "C NMR chemical shift assignments of trans-and cis-10-chlorodecal-2-ones were based on 2D COSY and HETCOR experiments. The spectra were measured either in CDCI, or in C,D, to optimize the spectral dispersion (ASIS effect). Selective spin decoupling experiments were also performed.

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