An X-ray study of the structure of a heattreated glassy carbon
โ Scribed by S. Ergun; R.R. Schehl; M. Berman
- Publisher
- Elsevier Science
- Year
- 1972
- Tongue
- English
- Weight
- 143 KB
- Volume
- 10
- Category
- Article
- ISSN
- 0008-6223
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โฆ Synopsis
The use of metal additives for the catalysis of graphitization of chars prepared by high temperature, high pressure ~rbonization of anthracene, phenanthrene or biphenyl has been investigated, In particular the extent and type of catalysis initiated by aluminum or beryllium has been examined, Quantitative X-ray measurements have been performed and this data is used to show the existence of at least two concurrent mechanisms of graphitization catalysis. Evidence for the preferential attack on the disorganized carbon by the graphitization catalyst has been found.
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X-ray diffraction patterns of eight carbon blacks produced from coals have been studied. Layer diameters, La, obtained from the (100) and (110) reflections ranged from 6 to 178, and the stack heights, L,, derived from the (002) reflections, ranged from 12 to 148. The above values compare with 2Oh an
An X-ray diffraction study of the carbons which were prepared from phenolformaldehyde resin, 3-methylphenol-formaldehyde resin and 3 \* 54imethylphenol-formaldehyde resin all heat treated in the temperature range from 900 to 3000ยฐC was carried out in order to find the relation between the graphitiza