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An X-ray Rietveld and infrared spectral study of the Na2(Mn1-xMx2+)Fe2+Fe3+(PO4)3 (x = 0 to 1 and M2+ = Mg, Cd) alluaudite-type solid solutions

✍ Scribed by Rondeux, M.; Hatert, F.

Book ID
127341301
Publisher
Mineralogical Society of America
Year
2010
Tongue
English
Weight
877 KB
Volume
95
Category
Article
ISSN
0003-004X

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An X-ray Rietveld and infrared spectral
An X-ray Rietveld and infrared spectral study of the Na2(Mn1-xMx2+)Fe2+Fe3+(PO4)3 (x = 0 to 1 and M2+ = Mg, Cd) alluaudite-type solid solutions
✍ Rondeux, M.; Hatert, F. 📂 Article 📅 2010 🏛 Mineralogical Society of America 🌐 English ⚖ 877 KB

Compounds of the Na 2 (Mn 1-x M 2+ x )Fe 2+ Fe 3+ (PO 4 ) 3 (M 2+ = Mg, Cd, Ca, Ni, Zn) alluaudite-type solid solutions were synthesized by hydrothermal techniques at 1 kbar, between 400 and 600 °C, and were investigated by X-ray powder diffraction and infrared spectroscopy. The site occupancy fact

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Several compounds of the (Na 1؊x Li x )CdIn 2 (PO 4 ) 3 solid solution were synthesized by a solid-state reaction in air, and pure alluaudite-like compounds were obtained for x ‫؍‬ 0.00, 0.25, and 0.50. X-ray Rietveld re5nements indicate the occurrence of Cd 2؉ in the M(1) site, and of In 3؉ in the