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An Original On-Column Oxidative Cleavage of Vicinal Diols Using Alumina/Potassium Periodate: Application to Sequential Oxidation/Horner–Emmons Reactions

✍ Scribed by Saada C. Dakdouki; Didier Villemin; Nathalie Bar

Publisher: John Wiley and Sons
Year: 2011
Tongue: English
Weight: 457 KB
Volume: 2011
Category: Article
ISSN: 1434-193X
DOI: 10.1002/ejoc.201100396

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## Abstract An on‐column solvent‐free oxidative cleavage reaction of vicinal diols by paraperiodic acid supported on silica gel at room temperature is described. The resulting pure carbonyl compounds are prepared in good to excellent yields with short reaction times. The cleavage reactions proceed