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An Isolable, Oxygen-Coordinated Silver(I) Complex of Dimethyl Diazomalonate: Synthesis and Characterization of [HB(3,5-(CF 3 ) 2 Pz) 3 ]Ag[OC(OCH 3 )] 2 CN 2 (Where Pz = Pyrazolyl)

✍ Scribed by Rasika Dias, H. V.; Polach, Sharon A.

Book ID: 127289273
Publisher: American Chemical Society
Year: 2000
Tongue: English
Weight: 33 KB
Volume: 39
Category: Article
ISSN: 0020-1669
DOI: 10.1021/ic0002521

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From a solution prepared by a reaction of Mo 2 (O 2 CCH 3 ) 4 with KTp\* (Tp\*= hydridotris(3,5-dimethylpyrazolyl)borate, HB(Me 2 Pz) 3 ), in diglyme at room temperature followed by addition of excess (CH 3 ) 3 SiBr to the red solution in refluxing THF, the complexes [HB(Me 2 Pz) 3 )BH][Br 3 Mo(m-Br