An investigation of solid-state phase transitions in 1- and 2-adamantanol by 13C CP-MAS NMR
β Scribed by Salman R. Salman; Robin K. Harris; John C. Lindon
- Publisher
- Elsevier Science
- Year
- 1991
- Tongue
- English
- Weight
- 314 KB
- Volume
- 179
- Category
- Article
- ISSN
- 0040-6031
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π SIMILAR VOLUMES
Using differential scanning calorimetry, we have investigated three difunctional cyanate monomers differing by their central group: bisphenol A dicyanate (BADCy), bisphenol E dicyanate (BEDCy), and hexafluorinated bisphenol A dicyanate (BAFDCy), to determine the effect of the central group on the mo
## Abstract A combination of solidβstate ^13^C CP/MAS NMR methods was used to study the rates of rotation of the phenyl group in 3,5βdimethylβ1βphenylhexβ1βynβ3βol. The methods used were __T__~1Ο~ measurements, lineshape analysis and 2D exchange spectroscopy over the temperature range 219β284 K. Th