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An in Situ Microcrystal X-ray Diffraction Study of the Synthetic Aluminophosphate Zeotypes DAF-1 and CoAPSO-44

✍ Scribed by Muncaster, Gavin; Sankar, Gopinathan; Catlow, C. Richard A.; Thomas, John Meurig; Bell, Robert G.; Wright, Paul A.; Coles, Simon; Teat, Simon J.; Clegg, William; Reeve, William


Book ID
126978363
Publisher
American Chemical Society
Year
1999
Tongue
English
Weight
152 KB
Volume
11
Category
Article
ISSN
0897-4756

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The synthesis of DPA-VPI-5 and TBA-VPI-5 and their phase transformation to AIPO4-8 have been studied by X-ray diffraction in situ. The synchrotron radiation-energy dispersive diffraction is shown to be able to monitor these two fast reactions in real time. The results indicate that nucleation may oc