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An improved synthesis of the antithyroid factor DL-goitrin

✍ Scribed by L. Brandsma; M. A. Keegstra; H. D. Verkruijsse; K. D. Bos

Book ID
104588890
Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
206 KB
Volume
107
Category
Article
ISSN
0165-0513

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## Abstract A convenient two‐step chemical synthesis of DL‐[2‐^13^C]‐glutamic acid from methyl acrylate and diethyl acetamidomalonate is described. Synthesis of the Michael adduct (III) was effected in quantitative yield by employing strong amino bases as catalysts. The reactivities of three such c