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An Improved Protocol for the Preparation of 5-Substituted Tetrazoles from Organic Thiocyanates and Nitriles

✍ Scribed by Vorona, Svetlana; Artamonova, Tatiana; Zevatskii, Yuri; Myznikov, Leonid


Book ID
121659529
Publisher
Thieme Medical Publishers
Year
2014
Tongue
German
Weight
212 KB
Volume
46
Category
Article
ISSN
0039-7881

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tris(2-perfluorohexylethyl)tin azide: A
✍ Dennis P. Curran; Sabine Hadida; Sun-Young Kim πŸ“‚ Article πŸ“… 1999 πŸ› Elsevier Science 🌐 French βš– 594 KB

The synthesis of a new fluorous tin azide, (C6FI3CH2CH2)3SnN 3, is reported and this reagent is used to make tetrazoles in both traditional and phaseswitching modes. In the traditional mode, the tin azide is reacted with nitriles followed by HCl cleavage to provide the tetrazoles and the fluorous ti