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AN EXPEDITIOUS ONE POT SYNTHESIS OF DIBENZO[a,g]FLUORENE

โœ Scribed by Banik, Bimal K.; Mukhopadhyay, Chhanda; Becker, Frederick F.


Book ID
127117842
Publisher
Taylor and Francis Group
Year
2001
Tongue
English
Weight
146 KB
Volume
31
Category
Article
ISSN
0039-7911

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An expeditious one-pot synthesis of diet
โœ Anna Klepacz; Andrzej Zwierzak ๐Ÿ“‚ Article ๐Ÿ“… 2002 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 48 KB

A general one-pot, purification-free synthesis of diethyl N-Boc-1-aminoalkylphosphonates has been developed. The procedure involves base-catalyzed Michael-type addition of sodium diethyl phosphite to N-Boc imines generated in situ by the action of sodium hydride on a-amidoalkyl-p-tolyl sulfones in t