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An efficient synthesis of (±) solenopsin A

✍ Scribed by Arévalo-García, Enzo B. (author)

Book ID
111682518
Publisher
Walter de Gruyter GmbH & Co. KG
Year
2012
Tongue
English
Weight
174 KB
Volume
18
Category
Article
ISSN
0793-0283

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Asymmetric synthesis of solenopsins A, B
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## Abstract Solenopsins A, B and C have been synthesized in enantiomerically pure forms from the corresponding __anti__‐1,5‐diols which have been obtained from glutaric anhydride by an asymmetric synthesis induced by chiral sulfoxides.

Enantiopure N-acyldihydropyridones as sy
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✍ Daniel L. Comins; Nezha Radi Benjelloun 📂 Article 📅 1994 🏛 Elsevier Science 🌐 French ⚖ 259 KB

The trans-pip&dine alkaloid, (-)-solenopsin A. was prepared in seven steps from readily available 4-~haxy-3\_(niiropropyrsilyllpyrfdin in 43% overall yield. The addition of organ~tallics to chiral 1-acylpyridinium salt 1 gives N-acyl-2-alkyl-23&hydta~4pyridones 2 with high diastereoselectivity.\*~ T