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An Efficient Synthesis of Diethyl 1-Aminoalkylphosphonate Hydrochlorides via the Intermediate Diethyl 1-Azidoalkylphosphonates

✍ Scribed by Gajda, Tadeusz; Matusiak, Maciej

Book ID
121235444
Publisher
Taylor and Francis Group
Year
1992
Tongue
English
Weight
307 KB
Volume
22
Category
Article
ISSN
0039-7911

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A general one-pot, purification-free synthesis of diethyl N-Boc-1-aminoalkylphosphonates has been developed. The procedure involves base-catalyzed Michael-type addition of sodium diethyl phosphite to N-Boc imines generated in situ by the action of sodium hydride on a-amidoalkyl-p-tolyl sulfones in t