An Efficient Synthesis of (+)-Decursinol from Umbelliferone.
β Scribed by Jung Ho Lee; Hyun Bae Bang; Su Young Han; Jong-Gab Jun
- Publisher
- John Wiley and Sons
- Year
- 2007
- Weight
- 12 KB
- Volume
- 38
- Category
- Article
- ISSN
- 0931-7597
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## Abstract 3β²βAminoβ3β²βdeoxyguanosine was synthesized from guanosine in eight steps and 58% overall yield. The 2β²,3β²βdiol of 5β²β__O__β[(__tert__βbutyl)diphenylsilyl]β2β__N__β[(dimethylamino)methylidene]guanosine was reacted with __Ξ±__βacetoxyisobutyryl bromide and treated with 0.5n NH~3~ in MeOH t