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An Efficient Synthesis of Bicyclic Amidines by Intramolecular Cyclization.

โœ Scribed by Naoya Kumagai; Shigeki Matsunaga; Masakatsu Shibasaki

Publisher
John Wiley and Sons
Year
2004
Weight
103 KB
Volume
35
Category
Article
ISSN
0931-7597

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complete (5-18 h; monitored by TLC). Then the solvent was removed under reduced pressure. The solid residue was directly purified by flash column chromatography on silica gel (eluent: petroleum ether/ ethyl acetate 7:3).