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An Efficient Strategy for the Synthesis of Endocyclic Enol Ethers and Its Application to the Synthesis of Spiroacetals

โœ Scribed by Fuwa, Haruhiko; Sasaki, Makoto

Book ID
120537769
Publisher
American Chemical Society
Year
2008
Tongue
English
Weight
212 KB
Volume
10
Category
Article
ISSN
1523-7060

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Water as an efficient medium for the syn
Water as an efficient medium for the synthesis of functionalized enol ethers
โœ Pascal Lemoine; Benoit Daoust ๐Ÿ“‚ Article ๐Ÿ“… 2008 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 167 KB

Herein we report an efficient method for synthesis of b-alkylated and b,b-dialkylated a-iodo enol ethers in water. Radical addition in aqueous medium of ethyl iodoacetate, iodoacetonitrile, and iodoacetamide to ynol ethers leads to a-iodo enol ethers with moderate to excellent yields and high stereo