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An efficient one-pot three component synthesis of 1,2-dihydro-1-arylnaphtho[1,2-e][1,3]oxazine-3-ones using montmorillonite K10 under solvent free conditions

✍ Scribed by Srinivas Kantevari; Srinivasu V. N. Vuppalapati; Rajashaker Bantu; Lingaiah Nagarapu


Publisher
Journal of Heterocyclic Chemistry
Year
2010
Tongue
English
Weight
117 KB
Volume
47
Category
Article
ISSN
0022-152X

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✦ Synopsis


Abstract

magnified image An efficient green protocol for the preparation of 1,2‐dihydro‐1‐arylnaphtho[1,2‐e][1,3]oxazine‐3‐ones employing a three‐component one‐pot condensation reaction of β‐naphthol, aromatic aldehyde, urea or thiourea in the presence of montmorillonite K10 clay under solvent free conditions has been described. The present procedure offers advantages such as shorter reaction time (<90 min), simple workup, excellent yields, recovery and reusability of catalyst. J. Heterocyclic Chem., (2010).


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