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An efficient, one-pot synthesis of trithiocarbonates from alcoholic tosylates using the Cs2CO3/CS2system

โœ Scribed by Devdutt Chaturvedi; Nisha Mishra; Amit K. Chaturvedi; Virendra Mishra

Book ID
106214271
Publisher
Springer Vienna
Year
2008
Tongue
English
Weight
66 KB
Volume
139
Category
Article
ISSN
0026-9247

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An efficient one-pot synthesis of N-alky
An efficient one-pot synthesis of N-alkyl carbamates from primary amines using Cs2CO3
โœ Ralph Nicholas Salvatore; Jeremy A Ledger; Kyung Woon Jung ๐Ÿ“‚ Article ๐Ÿ“… 2001 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 127 KB

A facile one-pot synthesis of N-alkyl carbamates is described. A primary amine, CO 2 , and an alkyl halide underwent a three-component coupling using cesium carbonate and tetrabutylammonium iodide (TBAI) giving rise to the resultant carbamate. In the presence of Cs 2 CO 3 , subsequent N-alkylation o