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An Efficient One-Pot Synthesis of 2-Hydroxyalkyl Dithiocarbamates

✍ Scribed by Cui, Jia-ling; Ge, Ze-mei; Cheng, Tie-ming; Li, Runtao


Book ID
120591671
Publisher
Taylor and Francis Group
Year
2003
Tongue
English
Weight
171 KB
Volume
33
Category
Article
ISSN
0039-7911

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Flavones were prepared using a one-pot procedure starting from the corresponding 2 0 -hydroxyacetophenones. The latter were treated with 3 equiv of aroyl chloride in wet K 2 CO 3 /acetone (1% w/w water) to afford a good yield of flavone and a smaller amount of 3-aroylflavone. Evidence was obtained t