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An efficient microwave-assisted synthesis furo[3,4-b]-[4,7] phenanthroline and indeno[2,1-b][4,7]phenanthroline derivatives in water

✍ Scribed by Feng Shi; Dianxiang Zhou; Shujiang Tu; Qingqing Shao; Chunmei Li; Longji Cao


Publisher
Journal of Heterocyclic Chemistry
Year
2008
Tongue
English
Weight
366 KB
Volume
45
Category
Article
ISSN
0022-152X

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✦ Synopsis


Abstract

magnified image

A series of furo[3,4‐b][4,7]phenanthroline and indeno[2,1‐b][4,7]phenanthroline derivatives were synthesized via a three‐component reaction of aromatic aldehydes, 6‐aminoquinoline and either tetronic acid or 1,3‐indanedione in water, under microwave irradiation without use of any catalyst. This green procedure offers several advantages including operational simplicity, clean reaction, and increased safety for small‐scale high‐speed synthesis.


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✍ Feng Shi; Dianxiang Zhou; Chunmei Li; Qingqing Shao; Longji Cao; Shujiang Tu 📂 Article 📅 2008 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 326 KB

## Abstract magnified image A series of benzo[__b__][4,7]phenanthroline derivatives were synthesized __via__ a three‐component reaction of aromatic aldehydes, 6‐aminoquinoline and either 1,3‐cyclohexanedione or dimedone in water under microwave irradiation without use of any catalyst. This method