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Amide Bond Formation Using an Air-Stable Source of AlMe3.

✍ Scribed by Andrew Novak; Luke D. Humphreys; Matthew D. Walker; Simon Woodward

Book ID
101993855
Publisher
John Wiley and Sons
Year
2006
Weight
25 KB
Volume
37
Category
Article
ISSN
0931-7597

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## Abstract We have achieved a 100 gram‐scale production of __anti__‐(2__S__,3__S__)‐β‐(__p__‐benzyloxy‐__m__‐chloro)phenyl‐__N__‐trifluoroacetyl‐L‐serine methyl ester (**1**) in high yield with high diastereo‐ and enantioselectivities based on a catalytic asymmetric Mukaiyama aldol reaction. The u