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Alternative Solid-Phase Strategies for the Efficient Labelling of Peptides with (Bathophenanthroline)ruthenium(II) Complexes

✍ Scribed by Rolf A. Kramer; Willi Bannwarth


Publisher
John Wiley and Sons
Year
2009
Tongue
German
Weight
320 KB
Volume
92
Category
Article
ISSN
0018-019X

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✦ Synopsis


Abstract

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To increase the flexibility for the insertion of highly sensitive and robust [Ru^II^(bathophenanthroline)] complexes into peptides, we have evaluated three different solid‐phase strategies (bathophenanthroline=4,7‐diphenyl‐1,10‐phenanthroline). Among these, insertion of the Ru‐complex‐modified lysine building block 9 turned out to be the method of choice (Scheme 5).