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Alternative, High‐Yield Synthesis of (E) ‐4‐Oxonon‐2‐enoic Acid from 2‐Methoxyfuran

✍ Scribed by Maras, Ahmet; Altay, Ahmet; Ballini, Roberto


Book ID
127048867
Publisher
Taylor and Francis Group
Year
2008
Tongue
English
Weight
101 KB
Volume
38
Category
Article
ISSN
0039-7911

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✍ Arie L. Gutman; John B. Campbell 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 French ⚖ 295 KB

## Abstract The synthesis of highly enriched C‐2 deuteriated and tritiated (E)‐5‐succinimido‐4‐oxo‐pent‐2‐enoic acid for use in enzymatic reduction is described. The starting materials 3‐methoxycarbonyl‐[3‐^2^H]propionyl chloride and 3‐methoxycarbonyl‐[3‐^3^H]propionyl chloride were prepared in hig