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Alkylation of 5-Amino-1,2,4-triazole with 1,2-Dibromoethane

✍ Scribed by M. I. Barmin; S. A. Gromova; I. I. Andrianova; V. V. Mel'nikov

Book ID
110312388
Publisher
Springer
Year
2001
Tongue
English
Weight
23 KB
Volume
71
Category
Article
ISSN
1070-3632

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4-Amino-3-(1,2,4-triazol-1-yl)-1H-1,2,4-triazole-5(4H)-thione
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In the molecule of the title compound, C 5 H 7 N 7 S, the essentially planar triazole ring and the 4-amino-5-mercapto-1,2,4-triazole moiety make a dihedral angle of 70.97 (5) . In the crystal structure, weak intermolecular N-HÁ Á ÁN and N-HÁ Á ÁS hydrogen bonds stabilize the packing.

Mass spectra of 1,2,4-triazolesβ€”II: Alky
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✍ A. J. Blackman; J. H. Bowie πŸ“‚ Article πŸ“… 1973 πŸ› John Wiley and Sons 🌐 English βš– 424 KB

## Abstract The mass spectra of monomethyl 1,2,4‐triazoles contain fragment ions produced by specific cleavage of the heterocyclic ring. A major fragmentation from many molecular ions involves the elimination of HCN, but loss of N~2~ is either very small or completely absent. No N or H scrambling o