Alkylation and rearrangement of lithiated 3-methyl-1,2-benzisoxazoles
β Scribed by Oliver, James E.; Waters, Rolland M.; Lusby, William R.
- Book ID
- 126187239
- Publisher
- American Chemical Society
- Year
- 1989
- Tongue
- English
- Weight
- 557 KB
- Volume
- 54
- Category
- Article
- ISSN
- 0022-3263
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Treatment of 2-methyl-2-hydroxy-6-alkyl-3,5-diacetylenes with powdered NaOH was used for the synthesis of terminal 1-alkyl-1,3-butadiynes that can be isolated (54-97%) or used in situ. In an attempt to increase the yields of some of the obtained products, different experimental conditions were studi