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Aliphatic1H and13C resonance assignments for the 26-10 antibody VLdomain derived from heteronuclear multidimensional NMR spectroscopy

✍ Scribed by Keith L. Constantine; Valentina Goldfarb; Michael Wittekind; Mark S. Friedrichs; James Anthony; Shi-Chung Ng; Luciano Mueller

Book ID
104679442
Publisher
Springer Netherlands
Year
1993
Tongue
English
Weight
913 KB
Volume
3
Category
Article
ISSN
0925-2738

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Nuclear Magnetic Resonance Spectroscopy
Nuclear Magnetic Resonance Spectroscopy for Structure Elucidation of Vitamin B12 Derivatives: Complete Interpretation of the13C-NMR Spectrum of Dicyanocobyrinic Acid Heptamethyl Ester and Partial Assignment of Its1H-NMR Spectrum
✍ Ernst, Ludger 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 English ⚖ 537 KB

## Abstract The ^13^C‐NMR chemical shifts of dicyanocobyrinic acid heptamethyl ester (**1**), an important corrinoid model compound, are correlated with those of some derivatives. Isotope effects on the ^13^C chemical shifts (over two to four bonds) are observed for the 10‐deuterio and the 10,13‐di