Advanced Organic Synthesis: A Laboratory Manual

✍ Scribed by Dmitry V. Liskin (Author); Penny Chaloner (Author)

• Publisher: CRC Press
• Year: 2015
• Leaves: 130
• Edition: 1
• Category: Library

✦ Synopsis

Laboratory experience equips students with techniques that are necessary for professional practice. Advanced Organic Synthesis: A Laboratory Manual focuses on a mechanistic background of key reactions in organic chemistry, gives insight into well-established trends, and introduces new developments in the field.The book features experiments performe

✦ Table of Contents

Diastereoselective Reduction of Estrone. Synthesis of 2,2-Dimethyl-4-pentene-1-amine. Protection of 2,2-Dimethyl-4-pentene-1-amine. Optimization of the Reaction Conditions for the Aminofluorination of N-(2,2-Dimethylpent-4-enyl)-2-toluenesulfonamide. Asymmetric Robinson Annulation. Formation of N- Benzylcinchonidinium Chloride from Cinchonidine. Chiral Resolution of BINOL (1,1`-bi-2-Naphthol) with N- Benzylcinchonidinium Chloride. Transesterification of Phosphatidylcholine and FAME Quantification. Green Chemistry: Solventless Sequential Aldol and Michael Reactions in the Synthesis of Krohnke Pyridine. Carbonyl Chemistry in a Multistep Synthesis. Multistep Synthesis of a Bioactive Peptidomimetic. Total Synthesis of a Natural Product: Caffeic Acid Phenethyl Ester (CAPE). Appendix: Essential Laboratory Techniques.

✦ Subjects

Bioscience;Biochemistry;Physical Sciences;Chemistry;Analytical Chemistry;Organic Chemistry